FIELD: chemistry.
SUBSTANCE: group of inventions relates to analytical chemistry and concerns a test system and a method of detecting salts of chloric acid, bromic acid and explosive compositions based thereon. Proposed method comprises sampling on sorption fibre, exposing sample to a strong acid and reaction with an aniline salt, reaction with a chemical reagent, providing presence of chloride ions. Further, method comprises use of a solid-phase sorbent, having strong acid properties. Sample for reaction is transported into a fixed layer of solid-phase sorbent with aqueous eluent. Test system which implements disclosed method, is a container with aqueous eluent, as well as a transparent micro-column, filled with a sorbent containing chemical reagents. End part of tube is covered with a soft sorption fibre, in contact with solid-phase sorbent forming a sampling surface.
EFFECT: using inventions provides high-accuracy of determination of a salt of chloric acid, bromic acid and explosive compositions based thereon.
8 cl, 1 dwg, 1 tbl, 1 ex
Title | Year | Author | Number |
---|---|---|---|
SET OF QUICK TESTS FOR PRESENCE OF EXPLOSIVE MATERIALS | 2015 |
|
RU2642599C2 |
METHOD OF EXPRESS-DETECTION OF EXPLOSIVE SUBSTANCES BASED ON ORGANIC PEROXIDES | 2013 |
|
RU2549446C2 |
METHOD AND KIT FOR DETECTING EXPLOSIVES CONTAINING CERTAIN OXIDANTS | 2005 |
|
RU2352936C2 |
METHOD FOR RAPID DETECTION OF INORGANIC AND ORGANIC PERCHLORATES | 2011 |
|
RU2484461C2 |
METHOD OF EXPRESS DETECTION OF EXPLOSIVES | 2013 |
|
RU2555758C2 |
METHOD OF PREPARING CHLORINE DIOXIDE (VARIANTS) | 1992 |
|
RU2104247C1 |
METHOD OF OBTAINING CHLORINE DIOXIDE | 2009 |
|
RU2519087C2 |
METHOD OF CHLORINE DIOXIDE PRODUCTION | 2010 |
|
RU2546659C2 |
METHOD FOR DETERMINING TRACE AMOUNTS OF NITRATE-IONS IN CHLORIDE STRONTIUM | 2016 |
|
RU2657443C1 |
REMOVING PERCHLORATE FROM CONCENTRATED SALT SOLUTIONS USING AMPHOTERIC ION-EXCHANGE RESINS | 2008 |
|
RU2482071C2 |
Authors
Dates
2017-04-13—Published
2014-07-18—Filed