FIELD: chemistry.
SUBSTANCE: method includes preparing a metal surface, preparing a solution with ultra-dispersed diamonds, and depositing the coating. In the method, a water suspension of ultra-dispersed diamonds is used, which is previously subjected to ultrasonic dispersion for 30-60 min, and in the preparation of the solution in distilled water, nickel sulfate, sodium acetate and acetic acid are dissolved, the solution is heated to a temperature of 87-90°C. The water suspension of ultra-dispersed diamonds is introduced into the resulting solution in the amount of 1-5 g/l, the ultrasonic dispersion of the solution is performed for 5 min, then sodium hipofosfit and thiourea are introduced, the ultrasonic dispersion of the solution is performed for 5 min. Then from the resulting solution containing, g/l: nickel sulfate - 20-30, sodium gipofosfit 10-25, sodium acetate - 10-15, acetic acid - 4-6 ml/l, thiourea - 0.001-0.003, ultra-fine diamonds - 1-5, at pH of 4.3-4.8 the coating is chemically precipitated on the prepared metal surface at a temperature of 87-90°C and a deposition rate of 0.15-0.2 mcm/min until the required thickness of the coating is obtained.
EFFECT: simplification of the technology of chemical nickel coating with ultra-dispersed diamonds by eliminating additional operations to maintain a certain size of ultra-dispersed diamond particles during the deposition of the coating, the possibility to obtain coatings with defined composition and properties.
1 tbl, 3 ex
Title | Year | Author | Number |
---|---|---|---|
COMPOSITE COATING BASED ON NICKEL WITH ULTRA-DISPERSED DIAMONDS | 2016 |
|
RU2638480C2 |
METHOD OF PRODUCTION OF METAL-DIAMOND CHEMICAL COATING | 2007 |
|
RU2375494C2 |
SOLUTION FOR CHEMICAL DEPOSITION OF COMPOSITE COATING | 2012 |
|
RU2509176C1 |
COMPOSITE METAL-DIAMOND COATING, METHOD OF ITS PRODUCTION, DIAMOND-CONTAINING ADDITIVE OF ELECTROLYTE AND METHOD OF ITS PRODUCTION | 2018 |
|
RU2699699C1 |
COMPOSITE METAL-DIAMOND COATING, METHOD OF ITS PRODUCTION, DISPERSE SYSTEM FOR DEPOSITION OF COMPOSITE METAL-DIAMOND COATING AND METHOD FOR ITS PRODUCTION | 2019 |
|
RU2706931C1 |
METHOD OF RECEIVING OF NICKEL-ADAMANTINE CHEMICAL COATINGS | 2007 |
|
RU2357002C1 |
METHOD OF COMPOSITION COATING RECEIVING | 2007 |
|
RU2357017C1 |
SOLUTION FOR CHEMICAL DEPOSITION OF COMPOSITION NICKEL COATINGS | 1995 |
|
RU2108416C1 |
SOLUTION USED FOR CHEMICAL DEPOSITION OF COMPOSITE NICKEL COATINGS | 2011 |
|
RU2465374C1 |
METHOD OF OBTAINING THE COATINGS | 0 |
|
SU1186283A1 |
Authors
Dates
2017-12-21—Published
2016-06-06—Filed