FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing trans-1,4,5,8-tetranitroso-1,4,5,8-tetraazadecalin by the condensation of glyoxal with ethylenediamine in the presence of sodium nitrite and acetic acid with subsequent dosage of the reaction mixture in dilute mineral acid, in which 30-40% sulfuric acid is used as mineral acid, and p-toluensulfonate is introduced into a mixture of glyoxal, ethylene diamine, sodium nitrite, acetic acid.
EFFECT: development of highly effective environmentally safe way of obtaining a compound.
2 cl, 1 tbl, 8 ex
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Authors
Dates
2018-01-25—Published
2017-01-23—Filed