FIELD: chemistry.
SUBSTANCE: method of producing elastomer composite grains comprises polymerizing one or more olefins in the presence of a catalyst with the formation of the elastomer polymer, obtaining a composite elastomer adhesive containing an elastomer polymer in the solvent, dispersing the nano-clay in the adhesive, treating the mixture of elastomer composite with water, steam, or their combination with obtaining solvent-depleted slurry comprising the elastomer composite grains. The solvent-depleted slurry contains less than 0.5 HSC of salt C8-C20-carboxylic acid. The elastomer composite grains are distributed in particle sizes, 74% of the particles have a size equal to 0.33 cm to 1.27 cm.
EFFECT: invention provides for the regulation of the grain size distribution in the emulsion or solution processes for the preparation of elastomer nanocomposites.
17 cl, 2 dwg, 7 ex
Title | Year | Author | Number |
---|---|---|---|
COMPOSITES OF FUNCTIONALISED ISOBUTYLENE-INORGANIC CLAY POLYMER AND METHOD USING AQUEOUS-ORGANIC EMULSION | 2006 |
|
RU2430118C2 |
ELASTOMERIC NANOCOMPOSITES, NANOCOMPOSITE COMPOSITIONS AND METHODS FOR PRODUCTION THEREOF | 2010 |
|
RU2561170C2 |
MICROLAYER COMPOSITES AND METHODS OF THEIR MANUFACTURING | 2004 |
|
RU2374076C2 |
ELASTOMERIC NANOCOMPOSITES, NANOCOMPOSITE COMPOSITIONS AND METHODS FOR PRODUCTION THEREOF | 2011 |
|
RU2592537C2 |
ELASTOMER NANOCOMPOSITES, NANOCOMPOSITE COMPOSITIONS AND METHODS FOR PRODUCTION THEREOF | 2011 |
|
RU2576596C2 |
THERMOPLASTIC ELASTOMERS AND VULCANISATES BASED ON ETHYLENE AND VINYL ALCOHOL COPOLYMERS | 2011 |
|
RU2570023C2 |
HOT-MELT PRESSURE-SENSITIVE ADHESIVE COMPOSITION AND ADHESIVE ARTICLE | 2006 |
|
RU2474598C2 |
GRAFTED POLYMERS INTENDED FOR DISPERSION OF GRAPHENE AND GRAPHITE | 2018 |
|
RU2759546C2 |
GRAPHITE-CONTAINING NANOCOMPOSITES | 2009 |
|
RU2519403C2 |
THERMOPLASTIC ELASTOMERIC COMPOSITION AND PREPARATION METHOD THEREOF | 2012 |
|
RU2599638C2 |
Authors
Dates
2018-02-02—Published
2013-05-03—Filed