IMPROVED MATERIALS OF HYDROPHOBIC AIRGELS Russian patent published in 2018 - IPC C01B33/158 C01B33/159 

Abstract RU 2668657 C1

FIELD: chemistry.

SUBSTANCE: group of inventions relates to inorganic chemistry. In order to obtain a reinforced airgel composition: a) precursor solution containing precursor materials of silica gel and a solvent is prepared; b) combining the precursor solution with the reinforcing material; c) transferring the silica gel precursor in solution to the gel composition to form a reinforced silica-based gel composition; d) recovering a portion of the solvent from the reinforced gel composition to produce a first reinforced airgel composition; e) exposing the first reinforced aerogel composition for heat treatment in an atmosphere with a reduced oxygen content at a temperature above 300 °C to obtain a second reinforced airgel composition. Additionally, hydrophobically bonded silicon is introduced into the first reinforced airgel composition prior to step d).

EFFECT: increase in hydrophobicity, absorption of liquid water, heat of combustion or the temperature of the onset of thermal decomposition of the airgel composition is provided.

20 cl, 19 ex, 1 tbl, 2 dwg

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RU 2 668 657 C1

Authors

Evans Owen

Dekraft Kathryn

Zafiropoulos Nicholas

Dong Wenting

Mihalcik David

Gould George

Melnikova Irene

Dates

2018-10-02Published

2015-10-02Filed