FIELD: chemistry.
SUBSTANCE: invention relates to the analytical chemistry and is intended for the non-volatile compounds content in volatile organic solvents, solutions, volatile compounds based extracts mass rapid determination. Non-volatile compounds content in non-aqueous media determining method consists is use of piezoquartz resonators as the scales, the analyzed sample microvolume application to the microvolume resonators electrodes, drying the sample and the nonvolatile sediment mass determining from the difference in the resonator oscillations frequency before application and after the sample drying, at that, according to the invention, a contour of polyvinyl acetate glue 1–2 mm thick is made on the quartz plate around the electrode, without covering the electrode, drying the contour and determining the piezoquartz resonator oscillation frequency before the analyzed sample application to the electrodes.
EFFECT: according to the invention the method allows to reduce the analysis time to 30 minutes; to increase the analysis performance – 4 samples / hour; reduce the sample volume for analysis to 1 mcl; increase the measuring elements durability – 1 sensor at least 10 measurements; significantly reduce the non-volatile compounds measuring instruments size.
1 cl, 2 dwg, 2 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF DETERMINING CONTENT OF SALTS IN MEDICINAL-TABLE MINERAL WATER | 2015 |
|
RU2607051C1 |
DEVICE FOR DETERMINATION OF DRY RESIDUE, NON-VOLATILE COMPOUNDS IN DRINKING, WASTE, NATURAL WATERS, FUELS, FOODSTUFFS | 2017 |
|
RU2678091C1 |
METHOD OF IDENTIFICATION OF GRANULATED HOPE SAMPLES BY ODOR WITH CHEMICAL SENSORS | 2017 |
|
RU2670651C9 |
METHOD OF ASSESSING QUALITY OF NITROGEN-CONTAINING MINERAL FERTILISERS WITH APPLICATION OF BIOSENSORS | 2013 |
|
RU2543687C1 |
CHEMICAL GAS SENSOR BASED ON HYDROXYAPATITES | 2017 |
|
RU2678771C1 |
METHOD FOR IDENTIFICATION AND SEMI-QUANTITATIVE DETERMINATION OF DIOCTYLPHTHALATE IN MIXTURE OF COMPOUNDS, RELEASED FROM PVC PLASTISOL | 2015 |
|
RU2603475C1 |
METHOD OF DETERMINING MICROCONCENTRATIONS OF AMMONIA VAPORS IN AIR | 2007 |
|
RU2319958C1 |
METHOD OF DETERMINING PHENOL IN AIR | 2010 |
|
RU2441231C1 |
METHOD OF OBTAINING DIAGNOSTIC INFORMATION ON THE SMELL OF THE SKIN | 2017 |
|
RU2679409C1 |
METHOD OF DETERMINING ACETONITRILE IN WORKING ZONE AIR | 2003 |
|
RU2237238C1 |
Authors
Dates
2019-02-18—Published
2017-11-27—Filed