NANODIAMONDS HAVING ACID FUNCTIONAL GROUP, AND METHOD FOR PRODUCTION THEREOF Russian patent published in 2019 - IPC C01B32/15 C01B32/28 B82B1/00 B82B3/00 B82Y40/00 

Abstract RU 2696439 C2

FIELD: chemistry.

SUBSTANCE: invention relates to nanotechnology. Nanodiamond obtained by detonation synthesis containing 0.15 mmol/g or more of acid functional groups, oxidative treatment is carried out with at least one oxidant selected from a group consisting of chromic acid, chromic anhydride, dichromic acid, manganic acid, perchloric acid, salts of said acids and hydrogen peroxide. Oxidative treatment can be carried out in the presence of sulphuric acid at temperature 130 °C or higher. If nanodiamonds do not contain acidic functional groups as a result of detonation synthesis, nanodiamond blend can be treated with mineral acid. Suspension of nanodiamonds after oxidative treatment can be subjected to disaggregating treatment. Obtained nanodiamonds have specific surface area of 150 m2/g or more and carboxyl functional groups with numerical density of 1 or more groups per square nanometer of the surface. Nanodiamond particles have d50 of 9 nm or less. High dispersibility of nanodiamond in dispersion media, for example in water, to obtain a stable dispersion.

EFFECT: invention can be used in production of lubricating, abrasive or insulating materials.

9 cl, 2 ex

Similar patents RU2696439C2

Title Year Author Number
SUSPENSION OF NANODIAMOND AGGREGATES AND SINGLE-NANO-SIZED NANODIAMOND DISPERSION 2015
  • Kojima, Ryouta
  • Kimoto, Norihiro
RU2700528C2
SURFACE-MODIFIED NANODIAMOND, A DISPERSED COMPOSITION OF NANODIAMONDS AND A METHOD FOR THE PRODUCTION OF SURFACE-MODIFIED NANODIAMOND 2020
  • Shiro, Daisuke
  • Kume, Atsushi
RU2780325C1
ZETA POSITIVE HYDROGENATED NANODIAMOND POWDER, ZETA POSITIVE SINGLE-DIGIT HYDROGENATED NANODIAMOND DISPERSION AND METHODS FOR PRODUCING SAME 2014
  • Myullyumyaki Vesa
RU2668437C2
METHOD FOR PRODUCING ZETA-NEGATIVE NANODIAMOND DISPERSION AND ZETA-NEGATIVE NANODIAMOND DISPERSION 2014
  • Myullyumyaki Vesa
  • Syuren Jesse
RU2681615C2
EXPLOSIVE COMPOSITION FOR DIAMOND SYNTHESIS 2021
  • Tsurui, Akihiko
  • Nishikawa, Masahiro
  • Mahiko, Tomoaki
  • Liu, Ming
RU2814424C1
CARBON-CONTAINING NANOPARTICLE AND METHOD OF ITS PRODUCTION 2009
  • Stavri Janev Stavrev
RU2424185C2
METHOD FOR CREATING SUSPENSION BASED ON DETONATION NANODIAMOND 2020
  • Plotnikov Vladimir Aleksandrovich
  • Makarov Sergej Viktorovich
  • Bogdanov Denis Grigorevich
  • Shutkin Aleksej Aleksandrovich
RU2757049C1
SORBENT REPRESENTING NANODIAMOND MATERIAL (VERSIONS), METHODS FOR OBTAINING AND APPLICATION THEREOF 2013
  • Ivanova Valerija Timofeevna
  • Ivanova Marina Viktorovna
  • Spitsyn Boris Vladimirovich
  • Trushakova Svetlana Viktorovna
  • Burtseva Elena Ivanovna
  • Isakova Aleksandra Aleksandrovna
  • Korzhanevskij Aleksandr Pavlovich
  • Denisov Sergej Aleksandrovich
  • Olesik Fedor Nikolaevich
RU2569510C2
METHOD OF PREPARING STABLE SUSPENSION OF DETONATION NANODIAMONDS 2008
  • Dolmatov Valerij Jur'Evich
  • Marchukov Valerij Aleksandrovich
  • Sushchev Vadim Georgievich
  • Veretennikova Marina Viktorovna
RU2384524C2
METHOD OF PURIFYING DETONATION NANODISPERSED DIAMONDS 2013
  • Marchukov Valerij Aleksandrovich
  • Kolodyazhnyj Aleksandr Leonidovich
  • Makarov Ivan Aleksandrovich
  • Korolev Konstantin Mikhajlovich
  • Sushshev Vadim Georgievich
RU2599665C2

RU 2 696 439 C2

Authors

Yamakawa, Akira

Dates

2019-08-01Published

2015-08-31Filed