METHOD FOR SELECTIVE PRODUCTION OF 1,2-BIS-STYRYLFULLERENE Russian patent published in 2020 - IPC C07C15/40 C07C15/20 C07C2/02 

Abstract RU 2712046 C1

FIELD: chemistry.

SUBSTANCE: invention relates to organic synthesis, specifically to a method of producing 1,2-bis-styrylfullerene. Substance of the method consists in fullerene (C60) with phenylacetylene in chlorobenzene in the presence of EtMgBr and Ti(OiPr)4, taken in molar ratio C60 : phenylacetylene : Ti(OiPr)4 : EtMgBr = 1:(2–4):(1–3):(8–12), at temperature of 80 °C for 10–30 minutes.

EFFECT: invention can be used as new promising materials, namely components of modern solar panels and field-effect transistors; obtaining 1,2-bis-styrylfullerene (1) with output of 10–80 %.

1 cl, 1 tbl, 1 ex

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RU 2 712 046 C1

Authors

Dzhemilev Usein Memetovich

Tuktarov Ajrat Ramilevich

Chobanov Nuri Mamedeevich

Dates

2020-01-24Published

2019-08-15Filed