FIELD: chemical or physical processes.
SUBSTANCE: invention relates to controlling production of polyisocyanates. Disclosed is a method of producing aromatic polyisocyanate in an apparatus for producing isocyanates containing a reactor section for a phosgenation reaction, where primary aromatic amine reacts with phosgene compounds in reactor section to obtain reaction product containing isocyanate, and where concentration of CO2 in gases coming from reactor section, measured and analyzed, and wherein the phosgenation reaction conditions are controlled when CO2 concentration in gases coming from the reactor section is higher than the background concentration of CO2. Also disclosed is version of proposed method for installation containing extraction section.
EFFECT: technical result is that the disclosed methods allow analyzing formation of by-products during the process and minimizing the amount thereof.
15 cl, 4 dwg, 1 ex
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Authors
Dates
2020-07-03—Published
2016-09-28—Filed