ELECTROLYTIC DEPOSITION OF LITHIATED TRANSITION METAL OXIDES, WHEN USING INITIAL PRECURSORS WITH LOW PURITY DEGREE Russian patent published in 2022 - IPC C25D17/10 C25D9/08 H01M10/525 

Abstract RU 2784167 C2

FIELD: electroplating.

SUBSTANCE: invention relates to the field of electroplating; it can be used in electrochemical energy storage devices including high-power and high-energy lithium-ion batteries. The method includes (a) immersion of a working electrode into a non-aqueous electrolyte containing a lithium source and a transition metal source, wherein the mentioned sources of both lithium and transition metal are characterized by a purity degree in the range from 50 to 95 wt. %; (b) electrical deposition of lithiated transition metal oxide (hereinafter – LTMO) on a surface of the working electrode from the electrolyte, at a temperature exceeding a melting point of the non-aqueous electrolyte; (c) removal of the working electrode from a bath, and (d) flushing of electrically deposited LTMO.

EFFECT: new method for synthesis of LTMO materials with reduced production costs is developed.

20 cl, 13 dwg

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RU 2 784 167 C2

Authors

Ates, Mehmet, N.

Busbee, John, D.

Kiggins, Chadd, T.

Cook, John, B.

Dates

2022-11-23Published

2019-05-23Filed