FIELD: organic chemistry.
SUBSTANCE: invention relates to the field of organic chemistry and is aimed at obtaining a linear oligophosphazene for plant protection in agriculture and forestry. Disclosed is a method for obtaining oligo[(N,N-dimethylethylenediamino)-(triazolyl)phosphazene], which consists in the fact that oligodichlorophosphazene in the medium of dried tetrahydrofuran and triethylamine interacts with triazole for 72 hours at a temperature of 23°C, followed by the addition of N,N- dimethylethylenediamine, then incubated for 72 hours at a temperature of 23°C, the solvent is distilled off, dialysis is carried out against water and dried at a pressure of 6 Pa and a temperature of 0°C.
EFFECT: invention provides an efficient method for producing oligo[(N,N-dimethylethylenediamino)-(triazolyl)phosphazene].
1 cl, 1 dwg
Title | Year | Author | Number |
---|---|---|---|
PHOSPHAZENE-CONTAINING EPOXY RESIN AND METHOD FOR ITS PRODUCTION | 2016 |
|
RU2639708C1 |
METHOD OF PRODUCING CYCLIC HALOPHOSPHAZENES BY REACTING HEXAALKYLDISILAZANES WITH HALOPHOSPHAZAPHOSPHONIUM SALTS | 2018 |
|
RU2729523C2 |
METHOD OF OBTAINING EPOXY RESIN, MODIFIED WITH EPOXYPHOSPHAZENES | 2013 |
|
RU2537403C1 |
METHOD OF PRODUCTION OF BETA-CARBOXYETHENYL PHENOXY-PHENOXYCYCLOPHOSPHAZENES | 2018 |
|
RU2662717C1 |
NOVEL PHOSPHAZENE APPLIED ON CARRIER CATALYST, NOVEL COMPOUND AND ITS APPLICATION | 2005 |
|
RU2340396C2 |
FIRE RETARDANT CATALYST FOR PRODUCTION OF POLYMERIC MATERIALS BASED ON POLYBENZOXAZINES, COMPOSITIONS WITH ITS USE | 2020 |
|
RU2756360C1 |
PHOSPHASE-CONTAINING OLIGOESTER ACRYLATE AND METHOD FOR ITS PRODUCTION | 2019 |
|
RU2743697C1 |
METHOD OF PRODUCING HEAT-RESISTANT NON-COMBUSTIBLE EPOXY BINDER BASED ON CYCLOPHOSPHAZENES | 2014 |
|
RU2589057C1 |
METHOD FOR PRODUCING 4-ALLYL-2-METHOXYPHENOXY-BETA-CARBOXYETHENYLPHENOXY-CYCLOTRIPHOSPHAZENES | 2019 |
|
RU2692686C1 |
METHOD FOR OBTAINING OLIHALOGENPHOSPHAZENES AND POLYHALOGENPHOSPHAZENES WITH REGULATED MOLECULAR MASS BY INTERACTION OF HALOGENOSPHORANES WITH HEXALCILDYSILAZANES | 2017 |
|
RU2645682C1 |
Authors
Dates
2023-02-14—Published
2022-06-22—Filed