FIELD: experimental physics and engineering instrumentation.
SUBSTANCE: invention relates to experimental physics and engineering instrumentation and concerns unwanted X-rays shielding in X-ray diffraction experiments for studying crystal structures of chemical compounds at high pressure and high temperature using high pressure chambers with diamond anvils equipped with a heating element. X-ray collimator is manufactured using a device consisting of two punches 1 and an insert 2 made of ceramic material placed between the punches, the profile of which follows the punches 1 profile. The insert 2 has a lenticular shape in the central part and a torus shape in the periphery, along the central axis of which holes are made in the punches 1 and in the insert 2 forming a single through hole, the diameter of which is equal to the outer diameter of metal capillary 5, which is placed in the through hole. The punches 1 are pressed to transfer the pressure created in the insert 2 to the capillary 5 to compress the capillary 5 and reduce its inner diameter in the compression zone. The capillary 5 is removed from the device and cut across the compression zone to obtain two identical collimators.
EFFECT: invention provides possibility to manufacture a collimator that allows diffraction experiments to be performed at high pressure and high temperature.
4 cl, 3 dwg
| Title | Year | Author | Number | 
|---|---|---|---|
| HIGH PRESSURE DEVICE WITH DIAMOND ANVILS | 2016 | 
									
  | 
                RU2623778C1 | 
| HIGH PRESSURE AND HIGH TEMPERATURE DEVICE WITH DIAMOND ANVILS | 2023 | 
									
  | 
                RU2833522C2 | 
| DIFFRACTOMETER ADJUSTING DEVICE | 0 | 
									
  | 
                SU1030709A1 | 
| RESONATOR FOR HIGH-PRESSURE ELECTRON PARAMAGNETIC RESONANCE MEASUREMENTS | 0 | 
									
  | 
                SU1636750A1 | 
| DEVICE FOR CONTROL OF X-RAY AND GAMMA BEAMS | 1993 | 
									
  | 
                RU2072575C1 | 
| METHOD FOR MANUFACTURING AND ASSEMBLY OF EXPLOSIVE CHARGES | 2009 | 
									
  | 
                RU2391325C1 | 
| COMPOSITE CONTAINING HIGH-ABRASIVE PARTICLES AND METHOD OF MANUFACTURING THEREOF | 1995 | 
									
  | 
                RU2135327C1 | 
| HIGH-TEMPERATURE SUPERCONDUCTING HYDRIDE AND METHOD FOR PRODUCTION THEREOF | 2020 | 
									
  | 
                RU2757450C1 | 
| RESONATOR FOR EPR MEASUREMENTS UNDER HIGH PRESSURES | 0 | 
									
  | 
                SU1086377A1 | 
| CAPILLARY NEUTRON-OPTICAL SYSTEM | 2007 | 
									
  | 
                RU2340023C9 | 
Authors
Dates
2023-02-21—Published
2022-11-16—Filed