METHOD FOR PRODUCING SOLID SULPHIDE ELECTROLYTE Russian patent published in 2023 - IPC H01M10/562 C01B17/22 C01B25/14 C01D15/00 H01M10/52 H01B13/00 H01B1/10 

Abstract RU 2804507 C2

FIELD: production of lithium-ion batteries.

SUBSTANCE: method for producing a sulphide-based solid electrolyte includes the first solution preparation step in which Li2S and P2S5 are mixed with each other in an organic solvent so that the Li2S/P2S5 molar ratio becomes from 0.7 to 1.5 to obtain a homogeneous Li-P-S solution; and a second solution preparation step which includes adding Li2S and SiS2 to an organic solvent to be mixed with them to obtain a homogeneous Li-Si-S solution. Next a solution mixing step is carried out in which the Li-P-S homogeneous solution and the Li-Si-S homogeneous solution are mixed with each other to obtain a homogeneous mixed solution. Then the resulting homogeneous mixed solution and Li2S are mixed with each other to obtain a suspension. This is followed by the drying step in which an organic solvent is removed from said suspension to obtain a precursor; and the heat treatment stage, at which the precursor is heated to 200-700°C to produce a sulphide-based solid electrolyte. An embodiment of the method for producing a sulphide-based solid electrolyte is proposed.

EFFECT: inventions make it possible to obtain a sulphide-based solid electrolyte with a low impurity content and stable characteristics.

11 cl, 4 dwg, 3 tbl, 3 ex

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RU 2 804 507 C2

Authors

Ito, Tomokhiro

Dates

2023-10-02Published

2020-02-25Filed