FIELD: chemistry.
SUBSTANCE: invention relates to a method for obtaining solid electrolyte based on LGPS having a certain crystal structure containing Li, P and S. The method for obtaining solid electrolyte based on LGPS is characterized by the presence of a stage at which a mixture of Li3PS4 crystals having a peak on the Raman spectrum at 420±10 cm-1 and Li4MS4 crystals (M is selected from a group consisting of Ge, Si and Sn) is subjected to heat treatment at 300-700°C; the presence of a stage at which Li3PS4 crystals having a peak on the Raman spectrum at 420±10 cm-1, Li2S crystals and sulfide crystals represented by the MS2 structure (M is selected from the group consisting of Ge, Si and Sn) are mixed, while preserving crystals and synthesizing a precursor; and a stage at which the precursor is subjected to heat treatment at 300-700°C.
EFFECT: high productivity, stable characteristics and a reduction in the formation of side products.
8 cl, 5 dwg, 8 ex
Authors
Dates
2021-09-08—Published
2018-03-16—Filed