FIELD: chemistry.
SUBSTANCE: invention relates to chemical engineering and can be used in making solid-state lithium-ion batteries. Method of producing highly dispersed lithium-conducting solid electrolyte Li1.3Al0.3Ti1.7(PO4)3 for lithium-ion batteries includes grinding, fine mixing and activation of a reaction mixture containing titanium oxide, lithium carbonate, aluminium hydroxide, ammonium dihydrophosphate and carbon; thermal treatment; cooling and dispersion of synthesized solid electrolyte. Addition of carbon to the mechanically activated reaction mixture leads to suppression of foaming of this mixture during the degassing process, after which the carbon is oxidised.
EFFECT: obtaining highly dispersed lithium-conducting solid electrolyte Li1.3Al0.3Ti1.7(PO4)3 with improved conducting properties using mechanical activation and foam suppressing additive (carbon).
5 cl, 10 dwg, 2 tbl, 8 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PRODUCING PARTICLES OF SOLID ELECTROLYTE LiAlTi(PO) (0,1≤x≤0,5) | 2012 |
|
RU2493638C1 |
METHOD OF PRODUCING POWDER OF SOLID ELECTROLYTE WITH HIGH CONDUCTIVITY ON LITHIUM ION | 2015 |
|
RU2583762C1 |
METHOD FOR PRODUCING COMPOSITE ANODE MATERIAL TiNbO/C FOR LITHIUM-ION BATTERIES | 2022 |
|
RU2799067C1 |
METHOD FOR PRODUCING ZIRCONIUM AND SODIUM PHOSPHATE SILICATE OF COMPOSITION NAZRSIPO WITH NASICON STRUCTURE | 2022 |
|
RU2780211C1 |
METHOD TO PRODUCE HIGHLY DISPERSED CATHODE MATERIALS LiFeMPO/C WITH OLIVINE STRUCTURE | 2010 |
|
RU2444815C1 |
ELECTROLYTE FOR SODIUM-ION ACCUMULATORS, METHOD OF ITS PRODUCTION AND ACCUMULATOR BASED ON IT | 2018 |
|
RU2707575C1 |
METHOD OF OBTAINING COMPOSITE CATHODE MATERIAL BASED ON NAV(PO)F FOR SODIUM-ION BATTERIES | 2020 |
|
RU2747565C1 |
METHOD FOR OBTAINING NaSn(PO) WITH NASICON STRUCTURE | 2021 |
|
RU2777643C1 |
METHOD OF PRODUCING SOLID ELECTROLYTE | 2019 |
|
RU2720349C1 |
COMPOSITE SOLID ELECTROLYTE FOR SOLID STATE LITHIUM ELECTROCHEMICAL DEVICES | 2021 |
|
RU2778549C1 |
Authors
Dates
2024-06-27—Published
2023-12-06—Filed