METHOD OF PRODUCING 5-NITROTETRAZOLE SALTS Russian patent published in 2016 - IPC C07D257/06 

Abstract SU 1841205 A1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing 5-nitrotetrazole salts via diazotation of 5-aminotetrazole with an alkali metal nitrite in a weakly acidic medium with subsequent extraction of end product using common techniques, wherein diazotation is carried out with an alkali metal nitrite taken in amount of 150-200 % against theoretically required, at temperature of 20-40 °C, followed by heating reaction mass to 80 °C and with further neutralisation with a base.

EFFECT: technical result is simple process of producing 5-nitrotetrazole and higher safety.

1 cl, 1 ex

Similar patents SU1841205A1

Title Year Author Number
SAFE METHOD FOR PRODUCING 2-METHYL-5-NITROTHETRAZOLE AND A MICROREACTOR FOR ITS IMPLEMENTATION 2018
  • Abiev Rufat Shovket Ogly
  • Svetlov Stanislav Dmitrievich
  • Ilyushin Mikhail Alekseevich
  • Pavlyukova Yuliya Nikolaevna
  • Nesterova Olga Mikhajlovna
  • Ostrovskij Vladimir Aronovich
RU2675599C1
METHOD FOR PRODUCING (5-NITROTETRAZOLATO-N) PENTAAMMINECOBALT (III) PERCHLORATE 2020
  • Varenitsa Viktor Ivanovich
  • Ageev Mikhail Vasilevich
  • Smirnov Andrej Vyacheslavovich
  • Fedotov Sergej Aleksandrovich
  • Vedernikov Yurij Nikolaevich
  • Nikolaev Yurij Viktorovich
  • Chuchupal Lyubov Nikolaevna
  • Ilyushin Mikhail Alekseevich
RU2767947C2
METHOD OF PRODUCING 2-ALKYL-5-NITROTETRAZOLES 1968
  • Soldatenko Dmitrij Sergeevich
  • Smirnov Sergej Petrovich
  • Kiseleva Anna Sergeevna
SU1841206A1
METHOD OF OBTAINING OF POTASSIUM SALTS OF RESIN ACIDS DERIVATIVES 2022
  • Popova Larisa Mikhailovna
  • Pochkaeva Evgeniia Igorevna
RU2811798C1
METHOD FOR PRODUCING 2-METHYLTHIO-6-NITRO-1,2-4-TRIAZOLO[5,1-C]-1,2,4-TRIAZIN-7-ONE SODIUM SALT DIHYDRATE POSESSING ANTIVIRAL ACTIVITY 2020
RU2741502C1
METHOD OF 2-ALKYL-5-NITRO-TETRAZOLE OR BIS (NITRO-TETRAZOLYL)-ALKANES PRODUCTION 1967
  • Soldatenko Dmitrij Sergeevich
  • Smirnov Sergej Petrovich
SU1841155A1
2,7-BIS[2-(DIETHYLAMINO)ETHOXY]FLUORENONE DIHYDROCHLORIDE (AMIXIN) PRODUCTION PROCESS 2006
  • Abuev Aleksandr Gebekovich
  • Kozubenko Sergej Pavlovich
  • Sakovich Gennadij Viktorovich
  • Snigur Gennadij Nikolaevich
  • Sysoljatin Sergej Viktorovich
RU2317974C1
METHOD OF PRODUCING 2,7-BIS-[2-(DIETHYLAMINO)ETHOXY]-FLUORENONE-9 DIHYDROCHLORIDE 2019
  • Sysolyatin Sergej Viktorovich
  • Kryukov Yurij Andreevich
  • Ishchenko Tatyana Andreevna
  • Shchurova Irina Anatolevna
  • Pocherevin Konstantin Sergeevich
RU2707176C1
METHOD OF SYNTHESIS OF DERIVATIVES OF 3-AMINO-2-MERCAPTOBENZOIC ACID (VARIANTS), DERIVATIVES OF BENZOTHIAZOLE AND METHOD OF THEIR SYNTHESIS 1996
  • Kunts Val'Ter
  • Jau Beat
RU2176241C2
AZO COMPOUNDS, INK COMPOSITION, METHODS FOR RECORDING AND COLORED MATERIAL 2011
  • Yoshimoto Takashi
  • Kawaguchi Akira
  • Ooshima Kenji
RU2583253C2

SU 1 841 205 A1

Authors

Smirnov Sergej Petrovich

Soldatenko Dmitrij Sergeevich

Kiseleva Anna Sergeevna

Dates

2016-10-20Published

1968-07-17Filed