PROCESS FOR SPLITTING 2,2-DIMETHYLCYCLOPROPANECARBOXYLIC ACID RACEMATE Russian patent published in 1994 - IPC

Abstract RU 2015953 C1

FIELD: organic chemistry. SUBSTANCE: the product: an optical isomer of 2,2-dimethylcyclopropanecarboxylic acid (α)2D

0 which has ∓ of 145 deg/(± 1) (without a solvent). Reagent 1: 2,2-dimethylcyclopropanecarboxylic acid ester or chloride. Reagent 2: mandelic acid methyl ester. Reaction conditions: fraction crystallization from alkane followed by alkaline hydrolysis, acidification and extraction from the nonpolar solvent. EFFECT: greater efficiency of the process. 4 cl

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RU 2 015 953 C1

Authors

Tomas Moil[De]

Dates

1994-07-15Published

1991-06-13Filed