FIELD: agriculture. SUBSTANCE: the product: trichlorfon (CH3O)2P(O)CH(OH)CCl3, C4H8Cl3O4P, m p 77-79 C. Reagent 1: chloral. Reagent 2: (CH3O)2PH(O). Reaction conditions: condensation is carried out in the liquid phase at a 2-fold excess of dimethylphosphite and the residence time of the reactants in the reaction zone for 2 to 14 min. EFFECT: improved properties of the title compound. 1 dwg
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Authors
Dates
1994-07-15—Published
1991-02-15—Filed