FIELD: powder preparing. SUBSTANCE: method involves mixing of 36.5020 g titanium butylate and 365 g butyl alcohol with density 0,810 g/cm2 with water content 2 wt.-%. Mixture is boiled in flask with reflux condenser for 0.5-2 h, metallic magnesium (2.5766 g) is added, cooled up to 50 C following by water addition (25 g by drops). Precipitate is separated by centrifugation and decantation, dried under vacuum at 60 C and annealed at 780-800 C for 1 h. White powder of the formula MgTiO3 showing high crystallinity degree is obtained. Method is simple and nonprolonged. EFFECT: improved method of product preparing.
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Authors
Dates
1995-03-27—Published
1992-07-02—Filed