FIELD: organic chemistry. SUBSTANCE: product - 2-N-methylamino-5-chlorobenzhydrylurea sulfate of the general formula , empirical formula is C15H16Cl30·H2SO4. Reagent 1: 2-N-methylamino-5-chlorobenzhydrol. Reagent 2: urea. Reaction conditions: urea and sulfuric acid were kept at 65-80 C, and 2-N-methylamino-5-chlorobenzhydrol is added to the mixture at ratio reagent 1:reagent 2:sulfuric acid = 5:7.5-20:20-25 (mmole). EFFECT: improved method of synthesis. 2 tbl
Title | Year | Author | Number |
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Authors
Dates
1995-04-20—Published
1991-04-08—Filed