4-AZIDONAPHTHALENE-1-SULFONYLCHLORIDE AS SEMIPRODUCT FOR SYNTHESIS OF (1′R,5′R) -3′-AZA-1′ -(2-AMINO-1,6-DIHYDRO-6-OXOPURINYL-9)-- 3′-DEOXY-3′- (4-AZIDONAPHTHALENE-1-SULFAMIDO) HEXOPYRANOSYL-- 6′-TRIPHOSPHATE TRILITHIUM SALT AS SPECIFIC PHOTOACTIVATED IRREVERSIBLE RNA-POLYMERASE INHIBITOR Russian patent published in 1995 - IPC

Abstract RU 2036902 C1

FIELD: organic chemistry. SUBSTANCE: product: 4-azidonaphthalene-1-sulfonylchloride, empirical formula is C10H6ClN3O2S, yield is 39%, m. p. is 114-116 C. Reagent 1: 4-azidonaphthalene-1-sulfoacid. Reagent 2: phosphorus pentachloride. Reaction condition: at 60-80 C. EFFECT: improved method of synthesis. 1 tbl

Similar patents RU2036902C1

Title Year Author Number
AZIDONAPHTHALENE -1-SULFONYLHYDRAZINES AS SEMIPRODUCTS FOR SYNTHESIS OF (1′R,5′R)-3′-AZA-1′- (2-AMINO-1,6-DIHYDRO-6-OXOPURINYL-9)-- 3′-DEOXY- 3′-(AZIDONAPHTHALENE-1-SULFAMIDO)-HEXOPYRANOSY- L-6′- TRIPHOSPHATES TRILITHIUM SALTS AS SPECIFIC PHOTOACTIVATED IRREVERSIBLE RNA-POLYMERASE INHIBITORS 1991
  • Khropov Ju.V.
  • Mishin A.A.
  • Seliverstov V.O.
  • Kulagin S.V.
  • Kochetkov S.N.
RU2036903C1
(1′R,5′R)-3′-AZA-1′- (2-AMINO-1,6-DIHYDRO-6- OXOPURINYL-9)-3′-DEOXY- 3′- (AZIDONAPHTHALENE-1-SULFAMIDO) -HEXOPYRANOSYL-6′-TRIPHOSPHA- TE TRILITHIUM SALTS AS SPECIFIC PHOTOACTIVATED IRREVERSIBLE RNA-POLYMERASE INHIBITORS 1991
  • Khropov Ju.V.
  • Mishin A.A.
  • Seliverstov V.O.
  • Kulagin S.V.
  • Kochetkov S.N.
RU2036928C1
HALOID-CONTAINING 3'-AMIDODERIVATIVES OF (1'R,5'R)-3' -AZA-1'-(2-AMINO -1,6-DIHYDRO -6-OXOPURINYL-9) -3'-DEOXYPYRANOSIDE AS SPECIFIC IRREVERSIBLE FLUORESCENT INHIBITORS OF RNA-POLYMERASE 1991
  • Khropov Ju.V.
  • Baranova L.A.
  • Tunitskaja V.L.
  • Kochetkov S.N.
RU2039065C1
LITHIUM SALTS OF (I'R,5'R)-3'-AZA-3'-(AZIDONAPHTHALINE-1- SULFAMIDO)-1'-(6-AMINOPURINYL-9)-3'-DEOXYHEXOPIRANOZYL- 6'-DI-OR TRIPHOSPHATES AS SPESIFIC PHOTOACTIVATED IRREVERSIBLE INHIBITORS OF Na, K-ADENOSINE TRIPHOSPHATASE 1997
  • Khropov Ju.V.
  • Mishin A.A.
  • Seliverstov V.O.
  • Kulagin S.V.
  • Lopina O.D.
RU2130943C1
5′-BENZOYLGUANOSINE DERIVATIVES AS SPECIFIC IRREVERSIBLE INHIBITORS OF RNA-POLYMERASE 1990
  • Khropov Ju.V.
  • Pinchuk N.Ja.
  • Baranova L.A.
  • Tunitskaja V.L.
  • Kochetkov S.N.
RU2035468C1
SALTS OF (1'R, 5'R)-3'-AZA-1'(6-AMINOPURINYL-9)-3'- DEOXYHEXOPYRANOSYL-6'-DIPHOSPHATE 3'-AMIDODERIVATIVES AS SPECIFIC FLUORESCENT INHIBITORS OF MYOSINIC ADENOSINE-5'- TRIPHOSPHATASE 1997
  • Baranova L.A.
  • Khropov Ju.V.
  • Pron'Ko G.M.
  • Petushkova E.V.
RU2131435C1
LITHIUM SALT OF N-CHLOROACETYLHYDRAZONE GUANOZINE-5'-TRIPHOSPHATE FOR SPECIFIC INHIBITION OF ADENYLATCYCLASE ACTIVITY SIMULATED WITH GUANYL NUCLEOTIDES 0
  • Khropov Yurij Valentinovich
  • Skurat Aleksandr Vladimirovich
  • Bogomolova Olga Arkadevna
  • Gulyaev Nikita Nikolaevich
SU1028675A1
METHOD FOR OBTAINING LITHIUM SALTS OF B-SUBSTITUTED BROMINE CONTAINING (IMIDAZO[2,1-I]PURINYL-3)-@@@-D-RIBOFURANOSYL-5'- PHOSPHATE 0
  • Khropov Yurij Valentinovich
  • Kulagin Sergej Viktorovich
SU1713904A1
DERIVATIVES OF TETRAFURAZANO-[3,4-B:3',4'-F:3'',4''-J:3''',- -4'''-N]-[1,4,5,8,9,12,13,16]-OCTAAZABICYCLO-[14,2,2]-EICOSA- -4,8,12-TRIENE AND METHOD OF THEIR SYNTHESIS 2000
  • Sheremetev A.B.
  • Betin V.L.
  • Judin I.L.
  • Kulagina V.O.
  • Khropov Ju.V.
  • Bulargina T.V.
  • Kots A.Ja.
RU2167161C1
5- OR 6-(N-PHTHALIMIDO)NAPHTHALENE-1-SULFOCHLORIDES AS SEMIPRODUCTS FOR SYNTHESIS OF SUBSTITUTED 5- OR 6-AMINONAPHTHALENE-1-SULFAMIDES 1989
  • Palajma A.I.
  • Butenas S.Ju.
  • Gauchene V.L.
  • Nedospasov A.A.
SU1702645A3

RU 2 036 902 C1

Authors

Kulagin S.V.

Seliverstov V.O.

Khropov Ju.V.

Mishin A.A.

Kochetkov S.N.

Dates

1995-06-09Published

1991-05-22Filed