FIELD: organic chemistry. SUBSTANCE: desired product methyl substituted sulfolene-3 has essential formula C5H8O25, its melting point is 62-63.2 C. Isoprene and pentadiene-1,3 being content of hydrocarbon C5 fraction of separation of gases of pyrolysis of benzine) is used as reagent 1. Liquid dioxide of sulfur is used as reagent 2. Reaction is carried out at 95-105 C under pressure 16-17 atm within 2-4. EFFECT: improves efficiency of the method. 5 cl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PRODUCTION OF CYCLIC SULFONE BUTADIENE-1,3 (SULFOLENE-3) | 1995 |
|
RU2065857C1 |
HIGH-OCTANE OXYGEN-CONTAINING COMPONENT | 1998 |
|
RU2132358C1 |
HIGH-OCTANE OXYGEN-CONTAINING COMPONENT | 1998 |
|
RU2128209C1 |
METHOD FOR PROCESSING COARSE VEGETABLE RAW MATERIAL FOR FODDER | 1994 |
|
RU2091038C1 |
CATALYST FOR SELECTIVE HYDROGENATION OF DIENE HYDROCARBONS | 2006 |
|
RU2292952C1 |
METHOD OF PRODUCING ISOPRENE | 2017 |
|
RU2654863C1 |
METHOD OF SYNTHESIS OF METHYLCYCLOHEXENES | 1988 |
|
SU1527842A1 |
METHOD OF PREPARING ALKYL-TERT-ALKYL ESTERS | 1999 |
|
RU2167142C2 |
METHOD OF PRODUCING HIGH-ANTIKNOCK GASOLINE COMPONENTS | 1994 |
|
RU2078793C1 |
ADJUSTER OF VISCOSITY OF POLYVINYL CHLORIDE PLASTISOL PASTES | 1994 |
|
RU2111988C1 |
Authors
Dates
1996-08-27—Published
1995-06-13—Filed