FIELD: organic chemistry. SUBSTANCE: product: bis-[b-chloroethyl]vinyl phosphonate of formula: b. Reagent 1: C6H11Cl2O3P. Reagent 2: alkali metal carbonate. Reaction conditions: at 90-130 C in the presence of catalyst resulting from reaction of aliphatic monohydric alcohol/ethylen glycol, glycerol or phenol with boron-containing reagent at molar ratio of 1-50:1. EFFECT: more efficient preparation process. 2 cl, 1 tbl
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Authors
Dates
1997-04-10—Published
1992-08-03—Filed