FIELD: organic chemistry, chemical technology. SUBSTANCE: product: 2-amidinothiourea. Reagent 1: dicyanodiamide. Reagent 2: ammonium hydrosulfite. Reaction conditions: pH = 7.8-10.0, at 35-90 C in the presence of sulfur. Yield is 25.3-43.6% at content of the basic substance 99%, not less. Synthesized compound is used in medicine and chemical industry. EFFECT: improved method of synthesis, increased yield. 2 cl, 1 tbl
Title |
Year |
Author |
Number |
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- Bojarintseva O.N.
- Kabanova I.A.
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- Alekseenko E.M.
|
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- Zemljakov N.D.
- Taranushich V.A.
|
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|
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- Shitova Eh.N.
- Islamgulova V.R.
- Shamsutdinova R.M.
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- Valitov R.B.
|
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- Donal'D Judzhin Batler
- Dzhodett Dzhejlej
- Tang Van Li
- Viliem Dzhon Iii Smit
- Dejvid Jurgen Vjustro
|
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- Belova V.M.
- Belovodskij V.P.
- Ozorova T.I.
- Serpukhovitin I.P.
- Davydovich D.V.
- Kirsanov A.T.
- Belov A.V.
|
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|
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- Vinogradov V.M.
- Tomchin A.B.
- Spivakova R.P.
- Katkov V.F.
|
SU1415725A1 |
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1996 |
- Junusov M.S.
- Tsyrlina E.M.
- Junusova S.G.
- Dokichev V.A.
- Savenko A.N.
- Istomin N.N.
- Lishtakov A.I.
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|
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