FIELD: organic chemistry, chemical technology. SUBSTANCE: method of synthesis of 3,4-dihydroxy-5-nitrobenzaldehyde involves interaction of 4-hydroxy-3-methoxy-5-nitrobenzaldehyde with the strong nucleophilic agent that can be obtained by interaction of aromatic mercapto-compound with the strong organic or inorganic alkaline metal base, for example, lithium hydroxide. Reaction is carried out at increased temperature using aprotonic polar solvent. Reaction is carried out preferably in inert atmosphere. EFFECT: improved method of synthesis. 6 cl
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Authors
Dates
1997-12-10—Published
1993-12-17—Filed