FIELD: production of sealing materials, compounds, sealing adhesives and similar products. SUBSTANCE: $$$-dioxydimethyl siloxanes having viscosity 10000 sSt are prepared by two-stepped heating products of hydrolysis of dimethyl dichlorosilane. The process is carried out in the presence of catalytically active hydroxide and/or potassium dimethyl siloxanolate in vacuum or by mixing of reaction mixture by bubbling with inert gas. At the first step temperature is maintained within 30-70 C range, at the second step temperature is maintained within 140-175 C range. EFFECT: simplified technology for production of product; decreased energy expense by realization of the method. 2 cl
Title | Year | Author | Number |
---|---|---|---|
GEL-LIKE ORGANOSILICON COMPOSITION | 1997 |
|
RU2127746C1 |
METHOD OF PREPARING ALKYL CHLOROMONOSILANES | 1996 |
|
RU2103273C1 |
METHOD OF PRODUCING ω, ω'-DIHYDROXYOLIGO-DIALKYLSILOXANES | 2010 |
|
RU2443726C2 |
UV-SOLIDIFIED ORGANOSILICON COMPOSITION FOR FIBRE LIGHT GUIDE COVERING | 1996 |
|
RU2118617C1 |
METHOD OF PREPARING PRODUCT OF ACID HYDROLYSIS OF ALKYL CHLOROSILANES | 1997 |
|
RU2130028C1 |
POLYORGANOSILOXANE COMPOSITION | 1997 |
|
RU2135535C1 |
METHOD OF PRODUCING OLIGODIMETHYLSILOXANES | 2013 |
|
RU2513022C1 |
METHOD OF PREPARING ALKOXYSILANES | 1999 |
|
RU2157375C1 |
METHOD OF PREPARING OLIGOALKYL SILOXANES | 1998 |
|
RU2160747C2 |
REACTOR FOR DIRECT SYNTHESIS OF ORGANOCHLOROSILANE | 1999 |
|
RU2162735C1 |
Authors
Dates
1997-12-27—Published
1996-08-23—Filed