FIELD: direct synthesis of methylchlorosilane; synthesis of polyorganosilaxane resin and silicones. SUBSTANCE: method is carried out by interaction of silicium with gaseous mixture of methane and chlorine at their molar ratio 1:0.1-0.40, the process takes place at 400-600 C. Thus mixture of trimethylchlorosilane. dimethyldichlorosilane and methyltrichlorosilane is prepared, mixture is separated by rectification. EFFECT: improved efficiency. 1 tbl
Title | Year | Author | Number |
---|---|---|---|
PROCESS FOR PREPARING CONTACT COMPOSITION FOR SYNTHESIS OF CHLORO- OR ORGANOCHLOROSILANES | 0 |
|
SU1131877A1 |
0 |
|
SU466239A1 | |
METHOD OF SYNTHESIS OF TRIMETHYLCHLOROSILANE | 1995 |
|
RU2099343C1 |
METHOD OF PREPARING ALKYL CHLOROMONOSILANES | 1996 |
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METHOD FOR PREPARING METHYLCHLOROSILANES | 2003 |
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METHOD OF METHYLCHLOROSILANES SYNTHESIS | 0 |
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SU1733435A1 |
METHOD OF TRIMETHYLCHLOROSILANE SYNTHESIS | 0 |
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SU1766924A1 |
METHOD OF ISOLATION OF TRIMETHYLCHLOROSILANE FROM ITS MIXTURE WITH SILICON TETRACHLORIDE | 1997 |
|
RU2119490C1 |
METHOD OF SEPARATING MIXTURE OF METHYLCHLOROSILANES AND METHYL CHLORIDE | 2012 |
|
RU2486193C1 |
METHOD FOR PRODUCTION OF METHYLCHLOROSILANES | 2001 |
|
RU2203900C2 |
Authors
Dates
1997-12-27—Published
1994-09-28—Filed