METHOD FOR JOINT PREPARATION OF MONO(CYCLOALKYL)DIMAGNESIUMBROMIDEFULLERENES(60) AND BIS(CYCLOALKYL)TETRAMAGNESIUMBROMID- EFULLERENES(60) Russian patent published in 1999 - IPC

Abstract RU 2136688 C1

FIELD: organic synthesis. SUBSTANCE: toluene solution of fullerene(60) interacts with excess of ether solution of α,ω- dimagnesium bromide in presence of zirconacene dichloride as catalyst for 10-20 hr under argon atmosphere and normal conditions to give products with yields 62-88%. EFFECT: extended synthetic possibilities. 1 tbl, 8 ex

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RU 2 136 688 C1

Authors

Dzhemilev U.M.

Nefedov O.M.

Ibragimov A.G.

Tomilov Ju.V.

Khafizova L.O.

Deeva E.A.

Ushakova Z.I.

Dates

1999-09-10Published

1998-04-29Filed