FIELD: industrial organic synthesis. SUBSTANCE: product, which is useful as antioxidant, is prepared via aminomethylation of 2,6-di-tert-butylphenol, followed by hydrogenolysis of intermediate Mannich base and isolation of final product by rectification and crystallization. The first stage is carried out in presence of 2,6-di-tert-butyl-4-methylcyclohexanol added to initial reaction mixture in amount of 1 to 25 wt %. EFFECT: simplified and reduced power consumption. 2 dwg, 5 tbl
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Authors
Dates
1999-09-20—Published
1997-09-08—Filed