2,6-DI-TERT-BUTYL-4-METHYLPHENOL (AGIDOL-1) PRODUCTION PROCESS Russian patent published in 1999 - IPC

Abstract RU 2137749 C1

FIELD: industrial organic synthesis. SUBSTANCE: product, which is useful as antioxidant, is prepared via aminomethylation of 2,6-di-tert-butylphenol, followed by hydrogenolysis of intermediate Mannich base and isolation of final product by rectification and crystallization. The first stage is carried out in presence of 2,6-di-tert-butyl-4-methylcyclohexanol added to initial reaction mixture in amount of 1 to 25 wt %. EFFECT: simplified and reduced power consumption. 2 dwg, 5 tbl

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RU 2 137 749 C1

Authors

Pantukh B.I.

Surkov V.D.

Logutov I.Ju.

Dates

1999-09-20Published

1997-09-08Filed