FIELD: chemical technology. SUBSTANCE: invention proposes a method of isolation of aniline at the content of nitrobenzene 0.0005 wt.-%, not above, from catalysates containing up to 0.5 wt.-% of nitrobenzene by rectification using phenylenediamines, diphenylamine, aminophenols as the separation promoter (separating agent). Rectification of dehydrated crude aniline is carried out at the residual pressure at the top of column 20-50 mm mercury column, at temperature in the column vat 95-145 C and the end trade product is obtained by the top of column. EFFECT: increased yield and purity of the end product. 10 ex
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Authors
Dates
1999-11-20—Published
1998-12-24—Filed