FIELD: organic chemistry. SUBSTANCE: invention relates to method of synthesis of mixing plasticizer consisting of 2,4-dinitro-2,4-diaza-pentane, 2,4-dinitro-2,4-diazahexane and 3,5-dinitro-3,5-diazaheptane. Synthesis is carried out by interaction of mixture of N,N'-dimethyl- and N,N'-diethylureas with fuming sulfuric acid followed by treatment of reaction mixture with formaldehyde and nitric acid at cooling. EFFECT: increased safety of process, facility, increased yield of end product. 1 tbl
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Authors
Dates
2000-05-10—Published
1999-04-20—Filed