FIELD: production of N-butyl xanthate. SUBSTANCE: method relates to production of collecting reagents fro flotation of ores of nonferrous metals, particularly, production of potassium or sodium N-butyl xanthate by reaction of carbon disulfide, potassium or sodium hydroxide, N-butyl alcohol in presence of water with their molar ratio of 1:1(2.5-3.0):(2.0-3.5) and temperature of 25-40 C with subsequent separation of xanthate by removal of liquid phase in vacuum. Process is carried out with fractional supply of N-butyl alcohol at stage of xanthation and dilution of reaction mass before drying with N-butyl alcohol and water taken in volume ratio of 1:(4.0-5.0), respectively. Technical result consists in simplification of process with preserved high yield of high quality product. EFFECT: higher efficiency. 2 ex
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Authors
Dates
2000-07-20—Published
1999-05-11—Filed