FIELD: fine organic synthesis, more particularly preparation of chlorinated aromatic sulfoxides. SUBSTANCE: 4,4'-dichlorodiphenyl sulfoxide is prepared by reacting sulfide with sulfuryl chloride. Diphenyl sulfide is first dissolved in carbon tetrachloride, and reaction is carried out in the presence of aluminium chloride at 0-5 C. Invention makes it possible to prepare 4,4'-dichlorodiphynyl sulfoxide by technologically simple method using available compounds with high yield (94%). Method uses simple equipment and has industrial application. EFFECT: more efficient preparation method.
| Title |
Year |
Author |
Number |
| METHOD OF PREPARING 4,4′-DICHLORODIPHENYL SULFIDE |
1996 |
|
RU2122538C1 |
| COPOLYMER OF STYRENE AND POLYHETEROARYLENE FOR POLYMERIC MATERIALS |
2000 |
- Vygodskij Ja.S.
- Sakharova A.A.
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- Sapozhnikov D.A.
|
RU2181366C2 |
| POLYACRYLAMIDE PRODUCTION PROCESS (VERSIONS) |
2001 |
- Lozinskij V.I.
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- Kalinina E.V.
|
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| COMPOSITION AS DEIODINATION CATALYST IN PRODUCTION OF HEXAFLUORO-1,2,3,4-TERACHLOROBUTANE AND HEXAFLUORO-1,2,3,4-TERACHLOROBUTANE PRODUCTION PROCESS |
2003 |
- Karimova N.M.
- Glazkov A.A.
|
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| METHOD OF PRODUCING SILOXANE-CONTAINING POLYIMIDES |
2005 |
- Vygodskij Jakov Semenovich
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- Said-Galiev Ehrnest Efimovich
- Ovchinnikov Anton Sergeevich
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- Vygodskij Ja.S.
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- Shaplov A.S.
|
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| COMPOSITION FOR PRODUCTION OF POLYISOCYANURATES FOR CONSTRUCTION MATERIALS |
1992 |
- Askadskij A.A.
- Pankratov V.A.
- Frenkel' Ts.M.
- Shvorak A.E.
- Goleneva L.M.
- Bychko K.A.
|
RU2061708C1 |
| COMPOSITION FOR PRODUCTION OF POLYMERIC STRUCTURAL MATERIALS BASED ON POLYISOCYANURATES |
2003 |
- Askadskij A.A.
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|
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|
RU2447094C2 |
| ARYLENE-BIS-(2-AMINOTHIOPHENE-3-CARBONITRILE(S) AS MONOMERS FOR PREPARING POLYAMIDES, POLYISOMETHINES AND POLYUREAS WITH PHENYLENE GROUPS |
2002 |
- Rodlovskaja E.N.
- Frolova N.G.
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- Nedel'Kin V.I.
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RU2230743C1 |
