FIELD: chemical processing of wood components, particularly, preparation of vanillin. SUBSTANCE: vanillin is prepared by oxidation of lignin-containing stock with oxygen in alkaline medicine in the presence of ortho-phenanetroline and azolignin of formula I: wherein L is polymeric matrix of lignin sulfate on heating followed by acidification of oxidate to pH of 2. EFFECT: increased yield of vanillin. 9 ex, 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD OF SYNTHESIS OF AROMATIC ALDEHYDES | 2000 |
|
RU2165920C1 |
METHOD FOR PRODUCTION OF AROMATIC ALDEHYDES FROM LIGNIN-CONTAINING MATERIAL | 2000 |
|
RU2164511C1 |
METHOD OF PREPARING VANILLIN | 1996 |
|
RU2117654C1 |
METHOD FOR PRODUCTION OF AROMATIC OXYALDEHYDES | 1994 |
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RU2078755C1 |
METHOD FOR ISOLATION OF VANlLLIN | 1993 |
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RU2078754C1 |
OXIDIZING AGENT FOR LIGNOSULPHONATES TO PRODUCE VANILLIN | 1996 |
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RU2117655C1 |
METHOD OF SYNTHESIS OF AROMATIC ALDEHYDES | 2001 |
|
RU2179968C1 |
METHOD OF PROCESSING SMALL-LEAVED WOOD | 2000 |
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RU2178405C1 |
PROCESS FOR PREPARING AROMATIC OXYALDEHYDES | 1992 |
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RU2057112C1 |
CHEMICAL WOOD PROCESSING METHOD | 1999 |
|
RU2158192C1 |
Authors
Dates
2001-10-27—Published
2000-09-15—Filed