FIELD: organic chemistry, chemical technology, radiolabeled compounds. SUBSTANCE: invention describes the compound N-[3H]-acetyl-D-glucosamine of the formula (I): and a method of its synthesis. Method involves the condensation reaction of D-glucosamine hydrochloride with [3H]CH3COOHNa in the presence of dicyclohexylcarbodiimide or metho-p-toluenesulfonate of 1-cyclohexyl-3-(2-morpholinoethyl)-carbodiimide or carbonylditriazole. EFFECT: improved method of synthesis, expanded assortment of labeled physiologically active compounds based on recommendation of conditions of their synthesis. 2 cl
Title |
Year |
Author |
Number |
HYDROCHLORIC ACID (N-NITRO)-ARGININE METHYL ESTER HIGHLY MARKED WITH TRITIUM |
1998 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2136641C1 |
DERIVATIVES OF SIALIC ACID HIGHLY LABELED WITH TRITIUM |
2001 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2190621C1 |
METHOD OF PREPARING QUATERNARY AMINE SALTS CONTAINING TRITIUM LABELLED AROMATIC RADICAL AT NITROGEN ATOM |
1995 |
- Shevchenko V.P.
- Mjasoedov N.F.
|
RU2089532C1 |
HIGHLY TRITIUM-LABELED ETHYL-(R)-1-(1-PHENETHYL)-1H-IMIDAZOLE-5-CARBOXYLATE AND METHOD FOR ITS PREPARING |
2001 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2206565C1 |
TRITIUM HIGHLY MARKED COENZYME A OR ACETYL COENZYME A |
1998 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2143416C1 |
FURAN DERIVATIVES HIGHLY LABELED WITH TRITIUM |
1998 |
- Shevchenko V.P.
- Mjasoedov N.F.
- Nagaev I.Ju.
|
RU2132331C1 |
METHOD OF SYNTHESIS OF 4-ETHYL-2,6,7-TRIOXA-1-PHOSPHOBICYCLO-[2,2,2]-OCTANE-1-OXIDE HIGHLY LABELED WITH TRITIUM OR DEUTERIUM AT ETHYL RADICAL |
1995 |
- Mjasoedov N.F.
- Shevchenko V.P.
- Faradzheva S.V.
- Nagaev I.Ju.
|
RU2108337C1 |
METHOD OF (1,5-(1,5-H)-D)-D-RIBOSE SYNTHESIS |
1987 |
- Mjasoedov N.F.
- Sidorov G.V.
- Kvjatkovskij Ju.G.
|
SU1513854A3 |
UNIFORMLY TRITIUM-LABELED 4,4-DIFLUORO-N-{(1S)-3-[3-(3-ISOPROPYL-5-METHYL-4H-1,2,4-TRIAZOL-4-YL)-8-AZABICYCLO[3,2,1]OCT-8-YL]-1-PHENYLPROPYL}CYCLOHEXANE CARBODIIMIDE |
2008 |
- Shevchenko Valerij Pavlovich
- Mjasoedov Nikolaj Fedorovich
- Nagaev Igor' Julianovich
|
RU2368613C1 |
METHOD OF SYNTHESIS OF HEXAPEPTIDE AMINO ACID FRAGMENTS MULTIPLE-LABELED WITH TRITIUM AT α-POSITION |
1988 |
- Zolotarev Ju.A.
- Zajtsev D.A.
- Mjasoedov N.F.
|
SU1736126A3 |