FIELD: organic chemistry, sugars. SUBSTANCE: synthesis is carried out by isotope exchange of 5-aldo-D-ribose or its 1,2-0-isopropylidene derivative with tritium in the presence of catalyst - palladium oxide on Al2O3 following by removal of protective group, if necessary. Under these conditions molar activity of the end product is increased up to 45 kKu/mmole. Radiochemical purity is 95% . EFFECT: enhanced molar activity and purity of product. 3 tbl
Title |
Year |
Author |
Number |
METHOD OF OBTAINING ALANINE MARKED BY RADIONUCLIDE |
1984 |
- Voronkov A.L.
- Kvjatkovskij Ju.G.
- Mjasoedov N.F.
- Sidorov G.V.
|
SU1140418A3 |
METHOD OF SYNTHESIS OF PROSTAGLANDINS TYPE e, OR THEIRS DERIVATIVES TYPE A, B, F, OR METHYL ESTERS OF PROSTAGLANDIN TYPE 1 MULTIPLE LABELED WITH TRITIUM |
1988 |
- Lazurkina T.Ju.
- Mjasoedov N.F.
- Nagaev I.Ju.
- Shevchenko V.P.
- Shram S.I.
|
SU1646252A3 |
METHOD OF PREPARING QUATERNARY AMINE SALTS CONTAINING TRITIUM LABELLED AROMATIC RADICAL AT NITROGEN ATOM |
1995 |
- Shevchenko V.P.
- Mjasoedov N.F.
|
RU2089532C1 |
METHOD OF SYNTHESIS OF HEXAPEPTIDE AMINO ACID FRAGMENTS MULTIPLE-LABELED WITH TRITIUM AT α-POSITION |
1988 |
- Zolotarev Ju.A.
- Zajtsev D.A.
- Mjasoedov N.F.
|
SU1736126A3 |
METHOD OF SYNTHESIS OF α-AMINO ACIDS LABELED WITH TRITIUM |
1986 |
- Zolotarev Ju.A.
- Dorokhova E.M.
- Kozik V.S.
- Zajtsev D.A.
- Mjasoedov N.F.
|
SU1436455A3 |
METHOD OF SYNTHESIS OF PROLINE HIGH-LABELED WITH TRITIUM |
1986 |
- Dorokhova E.M.
- Zolotarev Ju.A.
- Kozik V.S.
- Mjasoedov N.F.
|
SU1432968A3 |
METHOD OF SYNTHESIS OF PURINE BASES LABELED WITH TRITIUM |
1986 |
- Mjasoedov N.F.
- Sidorov G.V.
- Voronkov A.L.
- Kvjatkovskij Ju.G.
- Ivan'Kova E.K.
|
SU1545504A3 |
METHOD OF OBTAINING D′-(5-H)-RIBOSE |
1983 |
- Kaminskij Ju.L.
- Akulov G.P.
- Patokina N.A.
|
SU1172234A1 |
METHOD OF TRITIUM LABELED COMPOUNDS SELECTED FROM CLASSES OF AMINO ACIDS, AMINES, AMINOSUGARS, SUGARS, PURINE AND PYRIMIDINE BASES AND NUCLEOSIDES, CARBOXYLIC ACIDS, NITROGEN-CONTAINING DERIVATIVES OF TETRAHYDROTHIOPHENE |
1987 |
- Zolotarev Ju.A.
- Zajtsev D.A.
- Mjasoedov N.F.
|
SU1774613A1 |
METHOD OF OBTAINING (METHYL-H) THYMIDINE |
1983 |
- Mjasoedov N.F.
- Sidorov G.V.
- Kvjatkovskij Ju.G.
- Ivan'Kova E.K.
|
SU1127280A3 |