FIELD: chemistry of organosilicon compounds, chemical technology. SUBSTANCE: invention describes method of synthesis of high-pure organosilicon disulfanes by two-stage reaction that involves interaction of elemental sulfur and alkaline metal anhydrous sulfide with halogenalkylalkoxysilane followed by addition of additional amount of alkaline metal sulfide. Invention provides synthesis of high-pure substance with high yield percent. EFFECT: improved method of synthesis, increased yield. 4 ex
Title | Year | Author | Number |
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METHOD FOR PREPARING ORGANOSILYLALKYLPOLYSULFANES | 2001 |
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RU2267494C2 |
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PROCESS FOR PRODUCING SULPHUR-CONTAINING ORGANOSILICON COMPOUNDS | 0 |
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SU900814A3 |
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RU2387659C2 |
Authors
Dates
2003-02-27—Published
1998-08-07—Filed