FIELD: chemistry of metalloorganic compounds.
SUBSTANCE: invention describes a method for preparing phenylchlorogermanates with some phenyl radicals at germanium atom. Method involves interaction of phenylchlorosilane and germanium tetrachloride in the presence of aluminium chloride at enhanced temperature wherein compounds of the general formula (C6H5)nSiCl4-n wherein n = 2, 3 are used as phenylchlorosilanes, and process is carried out at temperature 105-150oC. Invention provides possibility for effective preparing diphenyldichlorogermanate.
EFFECT: improved preparing method.
1 tbl, 2 ex
| Title |
Year |
Author |
Number |
| GRIGNARD METHOD WITH INCREASED DIPHENYLCHLOROSILANE CONTENT |
2004 |
|
RU2354660C2 |
| PROCESS FOR PREPARING PHENYL- AND METHYLPHENYLCHLOROSILANES |
1991 |
- Vereninov G.M.
- Endovin Ju.P.
- Mironov V.F.
- Baturova S.A.
- Fel'Dshtejn N.S.
- Chekrij E.N.
|
RU2015982C1 |
| METHOD OF PREPARING TRIPHENYL SILANOL |
1999 |
- Zhun' V.I.
- Zhun' A.B.
- Polivanov A.N.
- Chernyshev E.A.
|
RU2174124C2 |
| GRIGNARD PROCESS WITH INCREASED OUTPUT OF DIPHENYLCHLOROSILANES AS PRODUCTS |
2004 |
- Ngujen Binkh Tankh
- Bedberi Kertis Dzhon
- Khamberg Rodzher Ehdvin
- Dzhejkob S'Juzan Mehri
- Ratkliff Sara Dzhejn
- Uoterman Dzhon Dennis
|
RU2345084C2 |
| CATALYST PREPARATION PROCESS AND ETHYLENE POLYMERIZATION AND ETHYLENE-ALPHA-OLEFIN COPOLYMERIZATION PROCESSES UTILIZING THIS CATALYST |
2004 |
- Mikenas T.B.
- Nikitin V.E.
- Zakharov V.A.
|
RU2257264C1 |
| METHOD OF PREPARING HALOGENMETHYLBENZOYL CYANIDES |
1995 |
- Izak Khejnts
- Kajl' Mikhaehl'
- Vol'F Bernd
- Vingert Khorst
- Vettling Tomas
|
RU2152926C1 |
|
0 |
|
SU424360A3 |
| PROCESS FOR HYDROXYALKYLATION OF AROMATIC CARBOCYCLIC ETHER, PROCESS FOR OXIDATION OF AROMATIC HYDROXYALKYLATED ETHER, VANILIN PRODUCTION PROCESS, AND ETHYLVANILIN PRODUCTION PROCESS |
1996 |
- Klod Moro
- Sil'Vi Razigad-Trussel'E
- Anni Finiel'
- Fransua Fazjula
- Loran Zhil'Ber
|
RU2169135C2 |
| METHOD OF OBTAINING VANADIUM-MAGNESIUM CATALYST OF ETHYLENE POLYMERISATION AND COPOLYMERISATION OF ETHYLENE WITH ALPHA-OLEFINS |
2012 |
- Mikenas Tat'Jana Borisovna
- Zakharov Vladimir Aleksandrovich
- Nikitin Valentin Evgen'Evich
|
RU2502560C1 |
| METHOD OF SYNTHESIS OF 1,1,1,2,2-PENTAFLUORO-3,3-DICHLOROPROPANE AND 1,1,2,2,3-PENTAFLUORO-1,3-DICHLOROPROPANE |
1991 |
- Khirokazu Aojama[Jp]
- Satoru Kono[Jp]
- Satosi Kojama[Jp]
|
RU2041193C1 |
