METHOD FOR PREPARING DIMETHYLETHANOLAMINE Russian patent published in 2006 - IPC C07C215/08 C07C213/04 

Abstract RU 2268254 C1

FIELD: organic chemistry, chemical technology.

SUBSTANCE: invention relates to a method for preparing dimethylethanolamine. Method involves interaction of anhydrous dimethylamine and ethylene oxide in two successive mixing reactors and displacing under enhanced temperature and pressure. Interaction is carried out under equilibrium pressure 6-13 atm in both reactors connected by gaseous phase. Dimethylamine and ethylene oxide are fed into reactor in the mole ratio = (3-6):1, and interaction is carried out up to achievement the concentration of ethylene oxide 1.4-5% at the mixing reactor outlet, and then the reaction mixture is fed into the displacing reactor. Method allows enhancing safety of the process, to provide high selectivity and increasing the output of the process in combination with simplicity of technological equipment.

EFFECT: improved preparing method.

1 tbl, 1 dwg, 4 ex

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RU 2 268 254 C1

Authors

Mikhajlova Tat'Jana Alekseevna

Nikushchenko Natal'Ja Trofimovna

Lugovskoj Sergej Anatol'Evich

Nagrodskij Mikhail Iosifovich

Lavrent'Ev Ivan Anatol'Evich

Dates

2006-01-20Published

2004-04-06Filed