FIELD: analytical methods.
SUBSTANCE: sample is heated together with pyrite to temperature Tn = (0.45...0.55)(TL-TS)+TS in container with magnesium oxide lock and, before hydrostatic weighing is performed, paraffin layer is deposited onto surface of sample. Summary content of gases is found in terms of following equation: where M1 and M1* are masses of sample before and after heating, respectively, g; M1' mass of sample after heating and deposition of paraffin, g; M2' mass of sample in water after heating and deposition of paraffin, g; V and V' are specific volume of distilled water at temperatures of corresponding weighing, cm3/g; Ta ambient temperature, °C; Th heating temperature of sample, °C; TL and TS are liquidus and solidus temperatures of test alloy, respectively, °C.
EFFECT: increased reproducibility and accuracy in testing aluminum alloy semimanufactured products for summary gas content.
1 dwg, 3 tbl
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Authors
Dates
2006-06-27—Published
2002-01-31—Filed