METHOD OF DETERMINING MOLECULAR MASS DISTRIBUTION OF ETHOXYSILOXANE OLIGOMERS IN HYDROLYZED AND NONHYDROLYZED ETHYL SILICATES Russian patent published in 2006 - IPC G01N30/26 

Abstract RU 2280252 C1

FIELD: analytical methods in the field of silicon-containing polymers.

SUBSTANCE: invention relates to manufacturing ceramic shell molds for precision metal molding according to molded templates using express control of binder for shell molds. Invention involves high-efficiency chromatographic columns filled with super-cross-linked polydivinylbenzene as sorbent and operated with absolute aliphatic alcohols, e.g. ethanol, as eluent. Calibration curve is preliminarily plotted using specially synthesized samples of individual ethoxysiloxane oligomers.

EFFECT: reduced determination time and avoided use of toxic eluents in chromatographic procedure.

2 cl, 2 tbl

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RU 2 280 252 C1

Authors

Pronin Aleksandr Jakovlevich

Khabarov Viktor Borisovich

Ospennikova Ol'Ga Gennadievna

Pikulina Larisa Vjacheslavovna

Antipin Lev Mikhajlovich

Larionov Oleg Georgievich

Dates

2006-07-20Published

2004-12-16Filed