METHOD OF DETERMINING HYDROGEN SULFIDE AND LIGHT MERCAPTANS IN CRUDE OIL, PETROLEUM DERIVATIVES, AND GAS CONDENSATE Russian patent published in 2006 - IPC G01N33/22 G01N33/26 G01N31/16 C01B17/16 C07C321/04 

Abstract RU 2285917 C1

FIELD: analytical methods in petroleum industry.

SUBSTANCE: invention relates to analytical checking of crude oil, petroleum derivatives, and gas condensate quality. 2 to 5g sample is thermostatically controlled at 50-70°C, while simultaneously hydrogen sulfide and light mercaptans are for 2-5 min displaced by inert gas or air into in series arranged absorption solutions, namely sodium carbonate solution for determining hydrogen sulfide and sodium hydroxide solution for determining light mercaptans. After complete withdrawal of hydrogen sulfide and light mercaptans, their quantitative content is determined by means of iodometric titration method.

EFFECT: extended range of analyzed products, increased determination accuracy, shortened analytical procedure, and enabled carrying out analyses not only in stationary laboratory without deviation from standardized procedures.

1 dwg, 1 tbl

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RU 2 285 917 C1

Authors

Sakhabutdinov Rifkhat Zinnurovich

Shatalov Aleksej Nikolaevich

Garifullin Rafaehl' Makhasimovich

Antonova Nadezhda Vasil'Evna

Dates

2006-10-20Published

2005-07-20Filed