FIELD: petroleum processing and petrochemistry.
SUBSTANCE: process comprises multistep compression of hydrocarbon feedstock pyrolysis gas, separation of water and liquid pyrolysis products, purification and drying of pyrolysis products, sorption drying of liquefied pyrolysis products formed in final pyrolysis, and multistep rectification. Sorption drying of liquefied pyrolysis products is carried out on porous solid sorbent comprising anhydrous calcium chloride, in particular 15-30% CaCl2, 70-85% Al2O3 or 15-30% CaCl2, 50-70% Al2O3, 15-20% SiO2, having loose density at least 0.6 g/cm3 and pore volume at least 0.5 cm3/g at temperature not higher than 40°C and excess pressure 1.9-4.0 MPa. Regeneration of sorbent is effected in flowing gas atmosphere containing at least 80 vol % methane, while cramping temperature to 150°C.
EFFECT: increased economical efficiency of separation allowing longer drying phases and enabling regeneration under milder conditions.
1 dwg, 3 ex
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Authors
Dates
2006-12-27—Published
2005-07-04—Filed