FIELD: chemical technology.
SUBSTANCE: invention describes a method for preparing immobilized β-cyclodextrin. Method involves pretreatment of organic and inorganic sorbents - polyvinyl alcohol and sorbitol based on silica with glutaraldehyde for incorporation of aldehyde group molecules into sorbents, washing out with water and dimethylsulfoxide on glass porous filter, drying on glass porous filter followed by addition of prepared sorbents to dimethylsulfoxide solution containing dissolved β-cyclodextrin in the ratio sorbent : β-cyclodextrin : dimethylsulfoxide = 1.0:(0.4- 2.0);10, respectively, stirring the prepared suspension at temperature 25-70°C for 30-180 min, washing out and drying. Method provides preparing an insoluble sorbent with immobilized β-cyclodextrin used for removing cholesterol or its derivatives.
EFFECT: improved preparing method.
5 ex
| Title | Year | Author | Number |
|---|---|---|---|
| SORBENT AND METHOD OF PREPARATION THEREOF | 2001 |
|
RU2203730C1 |
| METHOD FOR PREPARING HEPARINS OF LOW MOLECULAR MASS | 2005 |
|
RU2295538C2 |
| METHOD FOR PRODUCING SORBENT USABLE FOR DETERMINING GLYCOSYLATED BLOOD PROTEINS | 2002 |
|
RU2229129C1 |
| SORBENT AND METHOD FOR ITS PRODUCTION | 1996 |
|
RU2094117C1 |
| BIOCATALYST AND METHOD FOR ITS PREPARING | 2002 |
|
RU2233327C2 |
| METHOD OF PREPARING CARRIER FOR IMMOBILIZATION OF AMINE-CONTAINING COMPOUNDS | 0 |
|
SU1789532A1 |
| SORBENT FOR REMOVAL OF IMMUNOGLOBULINS | 2008 |
|
RU2389022C2 |
| CROSS-LINKED POLYVINYL ALCOHOL WITH THE IMMOBILIZED META-AMINOPHENYLBORONIC ACID AS A SORBENT FOR GLYCOSYLATED HEMOGLOBIN ASSAY BY AFFINITY METHOD | 1995 |
|
RU2093525C1 |
| 3,3',5,5'-TETRAMETHYL BENZIDINE HYDROCHLORIDE SUBSTRATE SOLUTION FOR ENZYME IMMUNOASSAY | 2017 |
|
RU2649556C1 |
| METHOD OF OBTAINING SORBENT FOR AFFINE CHROMATOGRAPHY | 0 |
|
SU1578138A1 |
