DICARBOXYLIC ACIDS PRODUCTION PROCESS Russian patent published in 2007 - IPC C07C51/31 C07C51/09 C07C55/14 C07C55/02 

Abstract RU 2296742 C2

FIELD: industrial organic synthesis.

SUBSTANCE: invention relates to improved process for production of dicarboxylic acids useful for various applications, for example as additive to various products, in manufacture of concrete, as well as monomers in polymer production. Process consists of oxidizing cyclohexane with oxygen or oxygen-containing gas in presence of oxidation catalyst and lipophilic-type oxidation solvent. Process comprises stage of extraction of dicarboxylic acids formed in oxidation stage, which extraction stage consisting in performing liquid-phase extraction of diatomic acids with the aid of first extraction solvent, wherein at least oxidation solvent and cyclohexane are insoluble, said extraction being carried out in countercurrent liquid-liquid extraction column.

EFFECT: enhanced process efficiency due to efficient diacid extraction stage and complete oxidation solvent recycling.

15 cl, 2 ex

Similar patents RU2296742C2

Title Year Author Number
CARBOXYLIC ACID SYNTHESIS METHOD 2006
  • Bonne Did'E
  • Petroff Sen-Arroma Romen
  • Rigini Sebast'En
  • Irelan Tan'Ja
  • Simonato Zhan-P'Er
RU2398757C2
METHOD OF OXIDIZING HYDROCARBONS INTO ACIDS 2001
  • Fashe Ehrik
RU2248345C2
METHOD FOR PRODUCTION OF DICARBOXYLIC ACIDS 2003
  • Bonne Did'E
  • Fash Ehrik
  • Simonato Zhan-P'Er
  • Verasini Serzh
RU2297997C2
ADIPIC ACID PRODUCTION PROCESS 2003
  • Bonne Did'E
  • Irelan Tan'Ja
  • Simonato Zhan-P'Er
RU2296743C2
METHOD FOR OXIDATION OF HYDROCARBON TO ACID 2002
  • Bonne Did'E
  • Fash Ehrik
  • Simonato Zhan-P'Er
RU2274633C2
METHOD OF OBTAINING ALKYLHYDROPEROXIDE 2011
  • Igerskhajm Fransuaz
  • Strejff Stefan
  • Verasini Serzh
RU2530896C2
METHOD OF RECIRCULATION OF CATALYST IN PROCESSES OF DIRECT OXIDATION OF CYCLOHEXANE TO ADIPIC ACID 1995
  • Mishel' Kostantini
  • Ehrik Fash
  • Daniel' Niver
RU2146240C1
METHOD FOR OXIDATION OF HYDROCARBONS 1998
  • Kostantini Mishel'
  • Fash Ehrik
RU2210562C2
METHOD FOR OXIDATION OF HYDROCARBON, ALCOHOL AND/OR KETONE 2001
  • Fash Ehrik
RU2235714C1
METHOD OF TREATING REACTION MIXTURES RESULTING FROM OXIDATION OF CYCLOHEXANE 1997
  • Ehrik Fash
  • Filip Lekont
  • Zhil'Ber Maren
RU2177937C2

RU 2 296 742 C2

Authors

Bonne Did'E

Amoro Daniel'

Simonato Zhan-P'Er

Ozh'E Frederik

Broglio Maria-In'Es

Dates

2007-04-10Published

2003-10-28Filed