FIELD: chemical technology.
SUBSTANCE: invention relates to a method for synthesis of hexafluorobut-1,3-diene. Process is carried out by the dehalogenation reaction of 1,2,3,4-tetrachlorohexafluorobutane with zinc in medium of high-boiling organic solvents chosen from the following order: diethylene glycol, polyethylene glycol, dimethyl ether, tetraethylene glycol, adipodinitrile, hexamethylphosphatriamide. Method provides simplifying process and absence of organic solvent and water in the final reaction product.
EFFECT: improved method of synthesis.
1 tbl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD FOR PREPARING HEXAFLUOROBUT-1,3-DIENE | 2005 |
|
RU2281278C1 |
| METHOD FOR PREPARING 1,2,3,4-TETRACHLOROHEXAFLUOROBUTANE | 2003 |
|
RU2246477C2 |
| HEAXAFLUOROBUTADIENE PRODUCTION PROCESS | 2003 |
|
RU2272017C2 |
| HEXAFLUOROBUTADIENE PRODUCTION PROCESS | 2002 |
|
RU2247104C2 |
| METHOD OF OBTAINING HEXAFLUOROBUTADIENE | 2006 |
|
RU2340588C2 |
| METHOD OF HEXAFLUOROBUTADIENE PREPARATION | 2007 |
|
RU2359951C1 |
| METHOD OF PRODUCING HEXAFLUORO-1,3-BUTADIENE AND INTERMEDIATE COMPOUND THEREOF | 2021 |
|
RU2815788C1 |
| METHOD FOR PREPARING 1,2,3,4-TETRACHLOROHEXAFLUOROBUTANE | 2003 |
|
RU2246478C1 |
| METHOD OF SIMULTANEOUSLY PREPARING CAPROLACTAM AND HEXAMETHYLENE DIAMINE | 1995 |
|
RU2153493C2 |
| METHOD FOR PREPARING 1,2,3,4-TETRACHLOROHEXAFLUOROBUTANE | 2005 |
|
RU2294917C1 |
