METHOD FOR PRODUCTION OF ALKYLHYDROXYALKYL CELLULOSE Russian patent published in 2007 - IPC C08B11/02 

Abstract RU 2309162 C2

FIELD: organic chemistry.

SUBSTANCE: invention relates to method for production of alkylhydroxyalkyl cellulose by interaction of cellulose with alkylation agent and hydroxyalkylation agent in presence of alkali, namely: a) cellulose is alkalified with 0.9-2.9 eq of alkali metal hydroxide/AGU introducing in form of aqueous alkali in presence of suspending agent containing haloalkyl wherein amount of haloalkyl is calculated according to the next formula: from [alkali metal hydroxide total per AGU] to [alkali metal hydroxide total per AGU plus 4.5]; b) alkali cellulose is react with alkylation agent and hydroxyalkylation agent such as one or more alkylene oxide at temperature of 65°C or more; c) alkali metal hydroxide is repeatedly added in form of aqueous alkali; and d) alkylhydroxyalkyl cellulose contained in reaction mixture is isolated and optionally purified.

EFFECT: mew method for production of alkylhydroxyalkyl cellulose.

7 cl, 36 ex, 8 tbl

Similar patents RU2309162C2

Title Year Author Number
METHOD OF PRODUCING METHYLHYDROXYPROPYL CELLULOSE, WHICH FORMS AQUEOUS SOLUTIONS OF DIFFERENT VISCOSITY 2023
  • Keller Iurii Petrovich
  • Nenashev Aleksei Borisovich
  • Kislykh Nikolai Vasilevich
RU2821789C1
CELLULOSE DERIVATIVES EXHIBITING GEL-LIKE RHEOLOGICAL PROPERTIES AND A METHOD FOR MANUFACTURING THEREOF 2003
  • Shleziger Khartvig
  • Kull' Arne Khenning
  • Klor Ehrik-Andreas
RU2321595C2
IMPROVED ALKYL HYDROXYALCYL CELLULOSE, METHODS FOR PRODUCTION AND APPLICATION THEREOF FOR CEMENT AND MORTARS 2014
  • Brash Kelli A.
  • Kauen Patrik Dzh.
  • Khon Vilfrid Adolf
  • Kindler Aleksander Adolfe
  • Nilles Vera Luize
RU2669615C1
IMPROVED COMPOSITION OF UNBLEACHED COTTON LINT, METHOD FOR ITS PREPARATION AND APPLICATION 2005
  • Dzhilett Pol S.
  • Maevich Tomas G.
  • Sau Ar'Jun S.
RU2396280C2
METHOD OF SYNTHESIS OF 3,7-DIALKYLXANTHINES 1993
  • Gerkhard Korb
  • Khans-Vol'Fram Flemming
RU2114847C1
METHOD OF OBTAINING CELLULOSE MIXED ETHERS 0
  • Sven Georg Lindenfors
  • Sven-Olof Jokhan Vestberg
SU1105118A3
REACTOR AND METHOD OF INDUSTRIAL PRODUCTION OF METHYLHYDROXYALKYL CELLULOSE AT IMPROVED ABILITY OF FORMING CLEAR SOLUTIONS 2002
  • Khol'Tketter Torsten
  • Mikhel' Shtefan
  • Zonnenberg Gerd
RU2320671C2
METHOD FOR PRODUCTION OF CELLULOSE HYDROXYALKYL ETHERS 2001
  • Andreev Ju.D.
  • Bondar' V.A.
  • Nikonova V.I.
RU2196778C1
WATERPROOFED ANIONIC CELLULOSE ETHERS 1998
  • Batelan Jan Gerardus
  • Dejk Berend Jan
  • Van Der Khorst Peter Marten
RU2191194C2
MODIFIED HYDROXYETHYL METHYLCELLULOSE FOR REINFORCED ADHESIVE FOR CERAMIC TILE AND METHOD FOR ITS PRODUCTION AND APPLICATION 2021
  • Teng Kun
  • Zhao Ming
  • Teng Bo
  • Li Qinghua
  • Jiang Aimei
  • Zhao Jianyu
  • Meng Zhaowu
RU2793325C1

RU 2 309 162 C2

Authors

Dannkhorn Vol'Fgang

Klor Ehrik-Andrehas

Kovollik Martin

Shleziger Khartvig

Pannek Jorn-Bernd

Dates

2007-10-27Published

2002-07-19Filed