Show metadata Hide metadata

(19)

(11)

2 360 916

(13)

(51)

IPC

C07D487/22(2006-01-01)

(21) (22)

Application

2008107776/04, 2008-02-28

(24)

Start date

2008-02-28

(22)

Actual filing date

2008-02-28

(45)

Published

2009-07-10

(72)

Inventor

Kalashnikov Aleksandr IvanovichSysoljatin Sergej ViktorovichLapina Julija TimofeevnaLobanova Antonina AlekseevnaKadulin Vladimir Viktorovich

(73)

Holder

Federal'Noe Gosudarstvennoe Unitarnoe Predprijatie Nauchno-Proizvodstvennyj Tsentr

METHOD FOR PREPARATION OF 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO[5,5,0,0,0]DODECANE Russian patent published in 2009 - IPC C07D487/22

Abstract RU 2360916 C1

FIELD: chemistry.

SUBSTANCE: invention refers to the method for preparation of the high-efficiency explosive 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5,5,0,0^3,11, 0^5'9]dodecane. 4,10-dibenzyl-2,6,8,12-tetraacetyl-2,4,6,8,10,12-hexaazatetracyclo[5,5,0,0^3,11,0^5,9]dodecane is hydrogenated in the mixture of formic and acetic acids, then obtained mixture of 4,10-diformyl-2,6,8,12-tetraacetyl-2,4,6,8,10,12-hexaazatetracyclo[5,5,0,0^3,11,0^5,9]dodecane and 4-formyl-2,6,8,12-tetraacetyl-2,4,6,8,10,12-hexaazatetracyclo[5,5,0,0^3,11,0^5,9]dodecane is nitrated in the crystalline form or in the mixture of formic and acetic acids.

EFFECT: substantial enhancing of the process feasibility and safety together with increase of the target product yield.

1 cl, 7 ex, 2 tbl

Similar patents RU2360916C1

Title	Year	Author	Number
METHOD OF 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO [5,5,0,0,0] DODECANE OBTAINMENT	2006	Kalashnikov Aleksandr Ivanovich Kadulin Vladimir Viktorovich Sysoljatin Sergej Viktorovich Chernikova Julija Timofeevna Lobanova Antonina Alekseevna	RU2355693C2
METHOD OF SYNTHESIS OF 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO-[5,5,0,0, 0]-DODECANE	2001	Sysoljatin S.V. Lobanova A.A. Chernikova Ju.T.	RU2199540C2
METHOD OF PRODUCING 2,6,8,12-TETRAACETYL-2,4,6,8,10,12-HEXAAZATETRACYCLO[5,5,0,03,11,05,9]DODECANE	2015	Kompaniets Ivan Igorevich Yakovlev Aleksej Andreevich Zolotukhina Irina Ivanovna	RU2610695C2
METHOD OF PRODUCING 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO[5,5,0,03,11,05,9]DODECANE	2015	Yakovlev Aleksej Andreevich Kompaniets Ivan Igorevich Zolotukhina Irina Ivanovna	RU2607517C1
METHOD OF PRODUCING CRYSTALLINE 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZA-TETRACYCLO[5,5,0,0,0]DODECANE HAVING GIVEN POLYMORPHOUS COMPOSITION	2010	Lapina Julija Timofeevna Lobanova Antonina Alekseevna Savitskij Sergej Aleksandrovich Zolotukhina Irina Ivanovna Kireeva Alena Valerievna	RU2452739C9
METHOD FOR PREPARING TETRAACETYLDIFORMYLHEXAAZAIZOWURTZITANE	2003	Gudkova N.I. Chernikova Ju.T. Sysoljatin S.V. Kalashnikov A.I. Lobanova A.A.	RU2266907C9
METHOD FOR OBTAINING 4,10-DIFORMYL-2,6,8,12-TETRAACETYL-2,4,6,8,10,12-HEXAAZATETRACYCLO[5,5,0,0,0]DODECANE	2021	Lapina Yuliya Timofeevna Kompaniets Ivan Igorevich Belyaev Vyacheslav Nikolaevich Zolotukhina Irina Ivanovna	RU2772755C1
4,10-BIS((±)-5-BENZOYL-2,3-DIHYDRO-1H-PYRROLO[1,2-A]PYRROLE-1-CARBONYL)-2,6,8,12-TETRAACETYL-2,4,6,8,10,12-HEXAAZATETRACYCLO[5,5,0,0,0]DODECANE AS ANALGETIC MEANS AND METHOD OF ITS OBTAINING	2014	Krylova Svetlana Gennad'Evna Amosova Evdokija Naumovna Zueva Elena Petrovna Razina Tat'Jana Georgievna Rybalkina Ol'Ga Jur'Evna Lopatina Ksenija Aleksandrovna Sysoljatin Sergej Viktorovich Kalashnikov Aleksandr Ivanovich Malykhin Valerij Viktorovich Dygaj Aleksandr Mikhajlovich Zhdanov Vadim Vadimovich	RU2558148C1
4,10-DI(ETHOXYACETYL)-2,6,8,12-TETRAACETYL-2,4,6,8,10,12-HEXAAZATETRACYCLO[5,5,0,0,0] DODECANE AS AN ANALGESIC AGENT AND A METHOD FOR PRODUCTION THEREOF	2020	Krylova Svetlana Gennadevna Poveteva Tatyana Nikolaevna Suslov Nikolaj Innokentevich Zueva Elena Petrovna Nesterova Yuliya Vladimirovna Afanaseva Olga Gennadevna Kulpin Pavel Valerevich Amosova Evdokiya Naumovna Razina Tatyana Georgievna Rybalkina Olga Yurevna Safonova Elena Andreevna Zhdanov Vadim Vadimovich Kalashnikov Aleksandr Ivanovich Bajbakova Olga Vladimirovna Bakholdina Lyubov Alekseevna Eremina Valeriya Valerevna Sonina Ekaterina Georgievna Kulagina Darya Aleksandrovna Sysolyatin Sergej Viktorovich	RU2736936C1
METHOD OF PRODUCING (-POLYMORPHIC MODIFICATION OF 2,4,6,8,10,12-HEXANITRO-2,4,6,8,10,12-HEXAAZATETRACYCLO [5,5,0,0]DODECANE	2011	Lapina Julija Timofeevna Lobanova Antonina Alekseevna Savitskij Sergej Aleksandrovich Zolotukhina Irina Ivanovna Kireeva Alena Valerievna	RU2447075C1

RU 2 360 916 C1

Authors

Kalashnikov Aleksandr Ivanovich

Sysoljatin Sergej Viktorovich

Lapina Julija Timofeevna

Lobanova Antonina Alekseevna

Kadulin Vladimir Viktorovich

Dates

2009-07-10—Published

2008-02-28—Filed