FIELD: chemistry.
SUBSTANCE: invention relates to method of obtaining water epoxide dispersion, used for impregnating concrete and wooden constructions in order to ensure their water-proofness, obtain anti-corrosion, decorative, electro-insulating coatings, as well as for impregnation of fabrics and for other purposes. Method consists in the following: epoxide component (A) and aliphatic difunctional compound (B) are brought into interaction with ratio A:B from 95:5 to 30:70 at temperature 50÷90°C during 1÷5 hours. Reaction is carried out in presence of tertiary amine or dimethylamine catalyst in amount from 0.01 to 5% of reagents weight until content of epoxide groups in component A decreases to from 5 to 70% of initial quantity. Epoxide ingredient represents mixture of cycloaliphatic or aliphatic resin with aromatic epoxide resin, containing ≥ 2 epoxide groups in molecule, with their ratio 3:97 to 97:3. Aliphatic difunctional compound represents compound selected from group including acid, alcohol, oxyacid. To obtained product of interaction initial component (A) is added with their ratio from 5:95 to 95:5. Further, mixture is mixed during 5÷25 minutes, four equal portions of distilled water are added with intervals from 5 to 75 minutes, and concentration of main substance is brought to 10÷70%.
EFFECT: obtaining stable water epoxide dispersion, containing product of interaction with residual epoxide groups, in absence of solvents and surface-active substances.
2 tbl, 11 ex
Title | Year | Author | Number |
---|---|---|---|
WATER-SOLUBLE EPOXY COMPOSITION | 2007 |
|
RU2365608C2 |
POLYMER COMPOSITION | 2011 |
|
RU2528681C2 |
EPOXIDE COMPOSITION | 2011 |
|
RU2478669C1 |
METHOD OF PRODUCING CURING AGENTS OF EPOXY RESINS | 2011 |
|
RU2488611C2 |
POLYMER COMPOSITION | 2011 |
|
RU2507227C2 |
POLYMER COMPOSITION | 2011 |
|
RU2478671C1 |
METHOD OF PRODUCING EPOXY RESIN CURING AGENTS | 2011 |
|
RU2507226C2 |
METHOD OF PRODUCING CURING AGENTS OF EPOXY RESINS | 2011 |
|
RU2478670C1 |
POLYMERIC COMPOSITE | 2001 |
|
RU2186802C1 |
POLYMER COMPOSITION | 2019 |
|
RU2769911C2 |
Authors
Dates
2009-08-27—Published
2007-10-11—Filed