METHOD OF CYCLOHEXYL-р-XYLOL HYDROPEROXIDE OBTAINMENT Russian patent published in 2009 - IPC C07C409/08 

Abstract RU 2370487 C1

FIELD: pharmacology.

SUBSTANCE: invention concerns cyclic hydrocarbons, particularly obtainment of cyclohexyl-p-xylol hydroperoxide, which can serve as source for simultaneous xylenol and cyclohexanol obtainment and as emulsion polymerisation initiator for unsaturated hydrocarbons. Cyclohexyl-p-xylol hydroperoxide is obtained by cyclohexyl-p-xylol oxidation by air oxygen at atmospheric pressure in the presence of N-hydroxyphthalamide catalyst in amount of 0.5-2.5 wt % and process temperature of 110-150°C for 1-3 hours till cyclohexyl-p-xylol hydroperoxide content reaches 9.8%.

EFFECT: reduced duration of oxidation process, reduced power cost.

1 cl, 2 tbl, 2 ex

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RU 2 370 487 C1

Authors

Koshel' Georgij Nikolaevich

Kurganova Ekaterina Anatol'Evna

Smirnova Elena Vladimirovna

Koshel' Sergej Georgievich

Plakhtinskij Vladimir Vladimirovich

Popovnina Antonina Nikolaevna

Dates

2009-10-20Published

2008-04-02Filed